Hydrothermal synthesis, structure and characterization of new NASICON related potassium iron (III) pyrophosphate | Zendy

G. S. Gopalakrishna | Zendy; B.H. Doreswamy | Zendy; M. Mahesh | Zendy; M. Mahendra | Zendy; M. A. Sridhar | Zendy; J. Shashidhara Prasad | Zendy; K. G. Ashamanjari | Zendy

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Hydrothermal synthesis, structure and characterization of new NASICON related potassium iron (III) pyrophosphate

Author(s) -

G. S. Gopalakrishna,

B.H. Doreswamy,

M. Mahesh,

M. Mahendra,

M. A. Sridhar,

J. Shashidhara Prasad,

K. G. Ashamanjari

Publication year - 2005

Publication title -

bulletin of materials science

Language(s) - English

Resource type - Journals

SCImago Journal Rank - 0.35

H-Index - 72

eISSN - 0973-7669

pISSN - 0250-4707

DOI - 10.1007/bf02711164

Subject(s) - pyrophosphate , materials science , monoclinic crystal system , hydrothermal circulation , potassium , hydrothermal synthesis , thermal stability , fast ion conductor , characterization (materials science) , crystallography , inorganic chemistry , crystal structure , chemical engineering , nanotechnology , chemistry , nuclear magnetic resonance , metallurgy , electrolyte , enzyme , electrode , engineering , physics

A new potassium iron (III) pyrophosphate was synthesized by hydrothermal technique and characterized by X-ray studies. The compound crystallizes in a monoclinic space group,P2 1/c, with cell parameters,a = 7 365(2) Å,b = 10017(2) Å,c = 8.214(1) Å,β = 106.50(1)° andZ = 4. The structure has tunnel-type cavities and are congenial for ion transportation through them. The compound exhibits moderate thermal stability.

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