High-performance liquid chromatographic determination of furfural and hydroxymethylfurfural in apple juices and concentrates | Zendy

Domingo Blanco Gomis | Zendy; María Dolores Gutiérrez-Álvarez | Zendy; L. Sopeña Naredo | Zendy; J. J. Mangas Alonso | Zendy

Open Access

High-performance liquid chromatographic determination of furfural and hydroxymethylfurfural in apple juices and concentrates

Author(s) -

Domingo Blanco Gomis,

María Dolores Gutiérrez-Álvarez,

L. Sopeña Naredo,

J. J. Mangas Alonso

Publication year - 1991

Publication title -

chromatographia

Language(s) - English

Resource type - Journals

SCImago Journal Rank - 0.427

H-Index - 67

eISSN - 1612-1112

pISSN - 0009-5893

DOI - 10.1007/bf02262465

Subject(s) - chemistry , chromatography , furfural , fruit juice , detection limit , 5 hydroxymethylfurfural , hydroxymethylfurfural , high performance liquid chromatography , extraction (chemistry) , cartridge , solid phase extraction , fructose , food science , organic chemistry , catalysis , mechanical engineering , engineering

A rapid and sensitive method for determining 2-furaldehyde (FUR) and 5-hydroxymethyl-2-furaldehyde (HMF) in apple juices and juice concentrates has been developed. The method for FUR and HMF involves the solid-liquid extraction of the juice by using a C-18 cartridge prior to reversed-phase separation with detection at 280 nm. The mobile phase was acetonitrile-water (8/92, v/v) at a flow rate of 1.0 ml/min. Recoveries from apple juices and juice concentrates spiked at different levels ranged from 94.1 to 104.0 (FUR) and 94.5 to 100.5 (HMF). The quantification limit for both, FUR and HMF, was 5 ppb.

The content you want is available to Zendy users.

Already have an account? Click here to sign in.

Having issues? You can contact us here

Accelerating Research