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C 12 H 13 ClO 4 , monoclinic,  C 2/ c  (no. 15),  a  = 35.310(2) Å,  b  = 5.9993(2) Å,  c  = 22.7422(8) Å, β = 98.692(4)°,  V  = 4762.3 Å 3 ,  Z  = 16,  R  gt  (F)  = 0.0397,  wR  ref  (F  2  )  = 0.1048,  T  = 153 K.

Crystal structure of 2-(4-chlorophenyl)-5-methyl-1,3-dioxane-5-carboxylic acid, C 12 H 13 ClO 4