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C 52 H 43 N 2 O 3 P 2 RhS, triclinic,  P 1̅ (no. 2),  a  = 10.6260(3) Å,  b  = 11.7305(3) Å,  c  = 19.6582(5) Å, α = 76.489(1)°, β = 82.027(1)°, γ = 64.848(1)°,  V  = 2154.4 Å 3 ,  Z  = 2,  R  gt  (F)  = 0.028,  wR  ref  (F  2  )  = 0.0722,  T  = 100 K.

Crystal structure of bis(triphenylphosphine)(carbonyl)(N-benzoyl-N'-(2-methyl-4-hydroxyphenyl)thioureato-κS,κN)rhodium(I), C 52 H 43 N 2 O 3 P 2 RhS