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C 22 H 23 Br 5 N 4 O 2 , monoclinic, P2/n (no. 13), a = 12.5980(6) Å, b = 6.0596(2) Å, c = 17.9790(8) Å, β= 105.253(2)°, V = 1324.2 Å 3 , Z = 2, R gt (F) = 0.0416, wR ref (F 2 ) = 0.1100, T = 293 K.

Crystal structure of bis(bromophenazone)hydrotribromide, (C 11 H 11 BrN 2 O) 2 HBr 3 , C 22 H 23 Br 5 N 4 O 2