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C 37 H 43 N 2 O 8 , triclinic, P1̄ (no. 2), a = 10.161(2) Å, b = 10.246(2) Å, c = 17.629(4) Å, α = 86.012(4)°, β = 78.092(4)°, γ = 73.458(4)°, V = 1721.4 Å 3 , Z = 2, R gt (F) = 0.0748, wR ref (F 2 ) = 0.2160, T = 293 K.

Crystal structure of meso-1,4-bis-(N-(endo-himoyl)-valinate)benzene hexane- hemisolvate, C 34 H 36 N 2 O 8 ·0.5C 6 H 14 , C 37 H 43 N 2 O 8