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C 42 H 83 Mo 6 N 3 O 20 , triclinic, P1̄ (no. 2), a = 12.683(3) Å, b = 12.878(4) Å, c = 19.433(6) Å, α = 74.27(2)°, β = 72.36(2)°, γ = 77.34(2)°, V = 2878.8 Å 3 , Z = 2, R gt (F) = 0.0664, wR ref (F 2 ) = 0.2268, T = 296 K.

Crystal structure of (Bu4N)2[Mo6O18N(o-CH 3 C 6 H 3 OOCCH 2 CH 3 )], C 42 H 83 Mo 6 N 3 O 20