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C 28 H 36 F 6 N 3 P, monoclinic, P2 1  (No. 4), a = 9.125(1) Å, b = 14.596(3) Å, c = 11.028(2) Å, β = 102.36(1)°, V = 1434.7 Å 3 , Z = 2,R gt (F) = 0.0783, wR ref (F2) = 0.1597, T = 293 K.

Crystal structure of (N,N',N"-trimethyl-N,N',N"-tris-(1-phenylethyl)- guanidinium hexafluorophosphate), C 28 H 36 F 6 N 3 P