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C 26 H 32 Mo 8 N 4 O 26 , monoclinic,  P 12 1 / c 1 (no. 14),  a  = 10.589(2) Å,  b  = 10.007(2) Å,  c  = 19.662(4) Å, β = 100.85(3)°,  V  = 2046.2 Å 3 ,  Z  = 2,  R  gt  (F)  = 0.023,  wR  ref  (F  2  )  = 0.056,  T  = 293 K.

Crystal structure of bis[(1,3-bis(4-pyridinium)propane)]- [β-hexacosaoxooctamolybdate(VI)], (C 13 H 16 N 2 ) 2 [Mo 8 O 26 ]