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C 30 H 24 Br 4 O 4 , monoclinic,  P 12 1 / c 1 (no. 14),  a  = 9.810(1) Å,  b  = 27.121(6) Å,  c  = 11.410(3) Å, β = 110.31(1)°,  V  = 2846.9 Å 3 ,  Z  = 4,  R  gt  (F)  = 0.068,  wR  ref  (F  2  )  = 0.126,  T  = 295 K.

Crystal structure of 5,11,17,23-tetrabromo-25,27-dihydroxy- 26,28-dimethoxycalix[4]arene, C 30 H 24 Br 4 O 4