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C 5 H 9 N 2 O 4 P, monoclinic,  C 12/ c 1 (no. 15),  a  = 13.462(4) Å,  b  = 10.209(3) Å,  c  = 12.582(4) Å, β = 110.96(3)°,  V  = 1614.8 Å 3 ,  Z  = 8,  R  gt  (F)  = 0.036,  wR  ref  (F)  = 0.046,  T  = 296 K.

Crystal structure of o-aminopyridinium dihydrogenmonophosphate, (NH 2 C 5 H 4 NH)[H 2 PO 4 ]