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C 14 H 14 N 2 NiO 6 , orthorhombic,  Pbca  (No. 61),  a  = 7.914(1) Å,  b  = 12.020(2) Å,  c  = 15.718(3) Å,  V  = 1495.3 Å 3 ,  Z  = 4,  R  gt  (F)  = 0.026,  wR  ref  (F  2  )  = 0.062,  T  = 293 K.

Crystal structure of diaqua-bis(pyridine)-μ2-squarato(1,3)-nickel(II), Ni(C 4 O 4 )(C 5 H 5 N) 2 (H 2 O) 2