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C 3 H 9 AlCl 6 NPSi, monoclinic,  P 12 1 / c 1 (No. 14),  a  = 15.541(3) Å,  b  = 12.615(2) Å,  c  = 16.210(3) Å, β = 116.128(2)°,  V  = 2853.3 Å 3 ,  Z  = 8,  R  gt  (F)  = 0.077,  wR  ref  (F  2  )  = 0.231,  T  = 100 K.

Crystal structure of trichloro(N-trimethylsilyl)phosphoraniminetrichloroaluminum, [(CH 3) 3 Si(N)PCl 3 AlCl 3 ]