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C 24 H 18 O 8 , monoclinic,  P 2 1 / n  (no. 14),  a  = 3.9930(7) Å,  b  = 26.483(5) Å,  c  = 10.3307(19) Å,  β  = 98.136(4)°,  V  = 1081.5(3) Å 3 ,  Z  = 2,  R  gt (F) = 0.0606,  wR  ref (F 2 ) = 0.1986,  T  = 293(2) K.

Crystal structure of tetramethyl 5,5′-(buta-1,3-diyne-1,4-diyl)diisophthalate, C 24 H 18 O 8