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C 14 H 16 N 6 NiS 4 , monoclinic,  P 2 1 / c  (no. 14),  a  = 8.817(16) Å,  b  = 10.172(17) Å,  c  = 10.043(17) Å,  β  = 97.77(4)°, V = 892(3) Å 3 ,  Z  = 2,  R  gt ( F ) = 0.0788,  wR gt (F 2 )  = 0.1962,  T  = 296 K.

Crystal structure of bis( N′ -((1 H -pyrrol-2-yl)methylene)-1-methylthio-methanethiohydrazido-κ 2 S , N )nickel(II), C 14 H 16 N 6 NiS 4