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C 68 H 104 O 4 , monoclinic,  P 2 1 / n  (no. 14),  a  = 19.4442(12) Å,  b  = 16.8522(11) Å,  c  = 38.048(3) Å,  β  = 92.400(1)°,  V  = 12456.4(14) Å 3 ,  Z  = 8,  R  gt ( F ) = 0.0488,  wR  ref ( F  2 ) = 0.1326,  T  = 153 K.

Crystal structure of 5,11,17,23-tetra( tert -butyl)-25,26,27,28-tetrahexoxycalix[4]arene, C 68 H 104 O 4