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C 18 H 15 N 6 O 7 Nb, monoclinic, P2 1 / c  (no. 14),  a  = 13.070(4) Å,  b  = 10.165(3) Å,  c  = 15.109(4) Å,  β  = 92.198(10)°,  V  = 2005.9(14) Å 3 ,  Z  = 4,  R  gt  (F)  = 0.0318,  wR  ref  (F 2 )  = 0.088,  T  = 100 K.

Crystal structure of tris( N -nitroso- N -oxyanilino-κ 2 O , O ′) oxidoniobium(V), C 18 H 15 N 6 O 7 Nb