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C 25 H 20 AsN 2 O 3 Rh, triclinic,  P -1 (no. 1),  a  = 9.2781(15) Å,  b  = 10.1405(15) Å,  c  = 13.303(2) Å,  α  = 99.789(5)°,  β  = 107.971(5)°,  γ  = 94.089(5)°,  V  = 1162.9(3) Å 3 ,  Z  = 2,  R  gt  (F)  = 0.0578,  wR  ref  (F  2  )  = 0.1833,  T  = 100(2) K.

Crystal structure of monocarbonyl( N -nitroso- N -oxido-phenylamine-κ 2 O , O ′)(triphenylarsine-κ As )rhodium(I), C 25 H 20 AsN 2 O 3 Rh