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C 6 H 5 N 11 O 6 , monoclinic,  P 2 1 / n  (no.  14),  a  = 13.463(5)  Å,  b  = 6.526(2) Å,  c  = 14.068(5) Å,  β  = 95.961(5)°,  V  = 1229.3(7) Å 3 ,  Z  = 4,  R  gt  (F)  = 0.0417,  wR  ref  (F  2  )  = 0.1067,  T  = 153 K.

Crystal structure of (E)-4,4′-(diazene-1,2-diyl)bis(1-nitro-1H-1,2,4-triazol-5(4H)-one)—acetonitrile (1:1), C 6 H 5 N 11 O 6