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C 26 H 24 N 2 NiO 6 , hexagonal,  P6522  (no. 179),  a  =  b  = 11.0161(4) Å,  c  = 33.1459(8) Å,  V  = 3483.5(9) Å 3 ,  Z  = 6,  R  gt  (F)  = 0.0376,  wR  ref  (F  2  )  = 0.0879,  T  = 295 K.

Crystal structure of bis(2-hydroxy-2-phenylacetato- κ 2 O , O ′)bis(pyridine- κ N )nickel(II), C 26 H 24 N 2 NiO 6