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C 12 H 14 O 4 , monoclinic,  C 2/ c ,  a  = 32.6674(8) Å,  b  = 6.0061(2) Å,  c  = 23.2786(6) Å,  α  = 90°,  β  = 103.368(2)°,  γ  = 90°,  V  = 4443.6(2) Å 3 ,  Z  = 16,  R  gt  (F)  = 0.0459,  wR  ref  (F  2  )  = 0.1412,  T  = 298(2) K.

Crystal structure of 5-methyl-2-phenyl-1,3-dioxane-5-carboxylic acid, C 12 H 14 O 4