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The CeCr 2 Al 20 -type (space group  Fd 3− m ) aluminum-rich intermetallic compounds  AT  2 Al 20  ( A  = Sr, Eu;  T  = Ti, V) were synthesized from the elements in alumina crucibles within evacuated sealed silica ampoules and characterized through X-ray powder patterns. SrTi 2 Al 20  ( a  = 1,475.25(6) pm) and SrV 2 Al 20  ( a  = 1,459.81(8) pm) are the first strontium-based aluminides with CeCr 2 Al 20 -type structure. The structures of Sr 0.836(2) V 2 Al 20 , Sr 0.961(1) V 2 Al 20  and Eu 0.964(2) V 2 Al 20  were refined from single crystal X-ray diffractometer data. Refinements of the occupancy parameters revealed defect formation on the 8 a  sites. In the strontium series, the lattice parameter scales with the occupancy parameter. Temperature dependent magnetic susceptibility data for the SrTi 2 Al 20  and SrV 2 Al 20  samples show diamagnetic and Pauli paramagnetic behavior, respectively.

Aluminum-rich cage compounds AT 2 Al 20 ( A = Sr, Eu; T = Ti, V)