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C 8 H 4 O 3 F 13 SK, monoclinic,  P 2 1 /c (no. 14),  a  = 27.550(3) Å,  b  = 16.0932(16) Å,  c  = 9.9834(10) Å,  β  = 96.686(4)°,  V  = 4396.3(8) Å 3 ,  Z  = 4,  T  = 100 K,  R   gt ( F ) = 0.0559,  wR ref   ( F   2 ) = 0.1609.

Crystal structure of potassium 1H,1H,2H,2H-perfluorooctanesulfonate, C 8 H 4 O 3 F 13 SK