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A modification to picric acid solutions has been undertaken to reveal the prior‐austenite grain boundaries in microalloyed steels as a result of elemental segregation. It has been found the maximum addition of sodium dodecyl sulphate plus hydrochloric acid to fully reveal both the prior austenite grain boundaries and the final post‐processed structures in these steels.

A new approach to etching low‐carbon microalloyed steels to reveal prior austenite grain boundaries and the dual‐phase microstructure