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In this article, a practical procedure for absolute intensity calibration for small‐angle scattering (SAXS) studies on liquid microjets is established. A gold nanoparticle suspension is used as standard so that the intercept at  Q  = 0 of the SAXS scattering curve provides a scaling reference. In order to obtain the most precise extrapolation at  Q  = 0, an extension of the Guinier approximation has been used, with a second‐order term in the fit that adapts to a larger  Q  range.

A dilute gold nanoparticle suspension as small‐angle X‐ray scattering standard for an absolute scale using an extended Guinier approximation