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Lead-free 0.95BaTiO 3 -0.05CaSnO 3  ceramics were synthesized by high energy ball milling (HEBM) assisted solid state reaction route. Calcination temperature and time for phase formation was optimized and found to be relatively less than other BaTiO 3 -doped system. X-ray diffraction (XRD) and Raman study were performed for phase examination of the synthesized material. Rietveld analysis confirmed double-phase co-existence of this 95/05 system at room temperature. Sintering temperature and time for better densification were optimized to be 1250°C for 3hr. From dielectric study it was found that ferroelectric-paraelectric phase transition temperature(T c, observed ≈ 55°C) was reduced considerably in compared to the pure BaTiO 3  system (T c ≈ 125°C). No relaxorbehaviour was found from dielectric study. Polarization vs. electric field hysteresis loop study showed the development of saturated hysteresis loops but the remnant polarization was found decreased compared to pure BaTiO 3  system.

iop conference series. materials science and engineering

Phase transition and ferroelectric properties study of lead-free 0.95BaTiO<sub>3</sub>-0.05CaSnO<sub>3</sub> ceramics synthesized by high energy ball milling assisted solid state reaction route

Phase transition and ferroelectric properties study of lead-free 0.95BaTiO3-0.05CaSnO3 ceramics synthesized by high energy ball milling assisted solid state reaction route

Phase transition and ferroelectric properties study of lead-free 0.95BaTiO₃-0.05CaSnO₃ ceramics synthesized by high energy ball milling assisted solid state reaction route