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Nickel-rich materials have been considered as promising cathode candidates for Li-ion batteries. In this work, the spherical Ni 0.8 Co 0.1 Mn 0.1 (OH) 2  precursor with good crystalline is synthesized via a hydrothermal method assisted with microfluidics. The effects of (NH 4 ) 2 CO 3  aqueous solution addition ratio and hydrothermal time on the formation of precursors are investigated comprehensively. The as-obtained precursors after optimization (hydrothermal time of 24 h and the concentration of the (NH 4 ) 2 CO 3  is 0.3 mol/L) display the spherical microstructure with homogenously distribution morphology, which can be clearly observed by scanning electron microscope. This work provides a rational route to controllably prepare the spherical Ni 0.8 Co 0.1 Mn 0.1 (OH) 2  precursors.

Synthesis of spherical Ni0.8Co0.1Mn0.1(OH)2 precursor via hydrothermal method assisted by microfluidics