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New azo reagent was synthesized by reaction dizonium salt Sulfadiazine with Pyrogallol. This product was characterized by FTIR, UV. Visible spectrophotometer and (XRD). Purity of the dye was checked by thin layer chromatography (TLC) using solvent system (Toluene-Methanol) (2:3). The melting point of the purified dye was measured in an open capillary tube. The results showed this compound have high levels of antibacterial activity.

X- ray diffraction Characterization of crystalline structure regent4(4-Sulphophenyl Azo) Pyrogallol