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10-Arylbenzo[ h ]quinolines were synthesized by cross-coupling of ethyl benzo[ h ]quinoline-10-carboxylate with arylboronic acids via group-directed Ni(0) catalyzation. The catalytic system combining Ni(COD) 2 (10 mol %) with PCy 3 (20 mol %) and  -BuOK (3 equiv) was optimal for the above transformations. A series of arylboronic acids reacted with ethyl benzo[ h ]quinoline-10-carboxylates for the production of various substituted 10-phenyl[ h ]quinolines in moderate and good yields under optimized reaction conditions.

Nickel(0)-Catalyzed Decarbonylative Cross-Coupling of Aromatic Esters with Arylboronic Acids via Chelation Assistance