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An acid‐responsive  N ‐heteroacene‐based material has been prepared, which shows a blue emission color in a film. The protonation of this material in a thin film gives rise to remarkable changes in luminescent color compared to that in solution states. As the protonation of  N ‐heteroacene molecules in films gradually occurs, their emission color can be tuned by adjusting the exposure time of the thin films to HCl vapor.

Acid‐Responsive N ‐Heteroacene‐Based Material Showing Multi‐Emission Colors