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W 18 O 49  with a tunable oxidation state was prepared by addition of NaNO 3  or NaBH 4  as a redox agent in the solvothermal system. The addition of redox agents has no influence on the crystallization of W 18 O 49 . The obtained W 18 O 49  structures keep their morphology as a bundle of nanowires with a regular hexagonal on the cross‐section. W 18 O 49  exhibits strong valence‐dependent absorption features in the near‐IR region. Reduced W 18 O 49  with more W 5+  has a higher concentration of oxygen vacancies, which enhances the localized surface plasmon resonance effect. Reduced W 18 O 49  exhibits a high photothermal conversion efficiency of 59.6 % and has good photothermal stability.

Photothermal Conversion of W 18 O 49 with a Tunable Oxidation State