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Premium polyoxometalates ! The organic functionalization of 3 d‐metalsubstituted polyoxometalates and the synthesis of new metal‐oxo clusters with accessible 3 d‐ and 4 f‐metal centers suitable for organic derivatization are discussed in this thesis. A total number of 39 compounds were structurally characterized, and their luminescent and magnetic properties analyzed. The solution behavior was studied by NMR spectroscopy, mass spectrometry, and light‐scattering techniques.

Systematic Studies on 3 d‐ and 4 f‐Metal Containing Polyoxometalates Suitable for Organic Derivatization