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Syntheses of 2‐([ 14 C]methyl)furan and 4‐oxo[5‐ 14 C]‐2‐pentenal
Author(s) -
Ravindranath Vijayalakshmi,
Burka Leo T.,
Boyd Michael R.
Publication year - 1984
Publication title -
journal of labelled compounds and radiopharmaceuticals
Language(s) - English
Resource type - Journals
SCImago Journal Rank - 0.432
H-Index - 47
eISSN - 1099-1344
pISSN - 0362-4803
DOI - 10.1002/jlcr.2580210804
Subject(s) - chemistry , furan , methyl iodide , lithium (medication) , medicinal chemistry , lithium iodide , organic chemistry , medicine , endocrinology , electrode , electrolyte
A simple one‐step syntheses of 2‐([ 14 C]‐methyl) furan and 4‐oxo‐[5‐ 14 C]‐2‐pentenal have been described. Carbon‐14 labeled 2‐methylfuran was synthesized by treatment of 2‐furyl lithium with 14 C‐methyl iodide, and 14 C‐acetylacrolein was obtained by peracid oxidation of labeled 2‐methylfuran.