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The synthesis of the 3‐hydroxyphenyl and 4‐hydroxyphenyl metabolites of 5,5‐diphenylhydantoin (Phenytoin) labelled with deuterium in either of the two phenyl rings and 5(4‐hydroxy‐[ 2 H 4 ]phenyl)‐5‐[ 2 H 5 ] phenylhydantion is described.