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Crystal growth, morphology, spectrographic characterization and thermal properties of 4,5‐bis(benzoylthio)‐1,3‐dithiole‐2‐thione
Author(s) -
Wang Xinqiang,
Xu Dong,
Zhang Guanghui,
Ren Quan,
Liu Weiliang
Publication year - 2008
Publication title -
crystal research and technology
Language(s) - English
Resource type - Journals
SCImago Journal Rank - 0.377
H-Index - 64
eISSN - 1521-4079
pISSN - 0232-1300
DOI - 10.1002/crat.200711116
Subject(s) - thermogravimetric analysis , raman spectroscopy , differential thermal analysis , morphology (biology) , diffraction , infrared spectroscopy , characterization (materials science) , materials science , absorption spectroscopy , powder diffraction , chloride , thermal analysis , crystal (programming language) , spectroscopy , crystallography , chemistry , infrared , analytical chemistry (journal) , thermal , optics , nanotechnology , organic chemistry , physics , programming language , quantum mechanics , biology , meteorology , computer science , genetics
Abstract Single crystals of 4,5‐bis(benzoylthio)‐1,3‐dithiole‐2‐thione (BBDT), were grown from methylene chloride and the growth morphology was deduced by the Bravais–Friedel Donnay–Harker (BFDH) model. The grown crystals were characterized by optical absorption, infrared, Raman and X‐ray powder diffraction spectroscopy. The thermal behavior of BBDT has been investigated by means of thermogravimetric analysis and differential thermal analysis measurements in air. (© 2008 WILEY‐VCH Verlag GmbH & Co. KGaA, Weinheim)