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We report the sustainable and efficient synthesis of a new type of quinoline derivatives bearing one or two SO 2 CF 3  groups. The protocol is metal‐, catalyst‐ and irradiation‐free, involves the use of readily available and stable precursors, and avoids the formation of side products. Also, the mild conditions of the process allow the tolerance of a wide range of functional groups.

A Convenient Formal [4+2] Heterocylization Route to Bis(triflyl)tetrahydroquinolines