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We report the efficient self‐templated formation of optically active 2,6‐bis(1,2,3‐triazol‐4‐yl)pyridine ( btp ) derived homocircuit [2]catenane enantiomers. This represents the first example of the enantiopure formation of chiral  btp  homocircuit [2]catenanes from starting materials consisting of a classical chiral element; X‐ray diffraction crystallography enabled the structural characterization of the [2]catenane. The self‐assembly reaction was monitored closely in solution facilitating the characterization of the  pseudo ‐rotaxane reaction intermediate prior to mechanically interlocking the pre‐organised system via ring‐closing metathesis.

Mechanically Interlocked Chiral Self‐Templated [2]Catenanes from 2,6‐Bis(1,2,3‐triazol‐4‐yl)pyridine (btp) Ligands