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The present work demonstrates the self‐organized formation of anodic molybdenum oxide nanotube arrays. The amorphous tubes can be crystallized to MoO 2  or MoO 3  and be converted fully or partially into molybdenum sulfide. Vertically aligned MoO  x  /MoS 2  nanotubes can be formed when, under optimized conditions, defined MoS 2  sheets form in a layer by layer arrangement that provide a high density of reactive stacking misalignments (defects). These core–shell nanotube arrays consist of a conductive suboxide core and a functional high defect density MoS 2  coating. Such structures are highly promising for applications in electrocatalysis (hydrogen evolution) or ion insertion devices.

angewandte chemie international edition

Aligned MoO  x  /MoS 2  Core–Shell Nanotubular Structures with a High Density of Reactive Sites Based on Self‐Ordered Anodic Molybdenum Oxide Nanotubes