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Abstract  The high‐pressure hydrogenation of commercially available anatase or anatase/rutile TiO 2  powder can create a photocatalyst for H 2  evolution that is highly effective and stable without the need for any additional co‐catalyst. This activation effect cannot be observed for rutile; however, for anatase/rutile mixtures, a strong synergistic effect can be found (similar to results commonly observed for noble‐metal‐decorated TiO 2 ). EPR and PL measurements indicated the intrinsic co‐catalytic activation of anatase TiO 2  to be due to specific defect centers formed during hydrogenation. These active centers can be observed specifically for high‐pressure hydrogenation; other common reduction treatments do not result in this effect.

Hydrogenated Anatase: Strong Photocatalytic Dihydrogen Evolution without the Use of a Co‐Catalyst