Fast Nucleation and Growth of ZIF‐8 Nanocrystals Monitored by Time‐Resolved In Situ Small‐Angle and Wide‐Angle X‐Ray Scattering | Zendy

Cravillon Janosch | Zendy; Schröder Christian A. | Zendy; Nayuk Roman | Zendy; Gummel Jeremie | Zendy; Huber Klaus | Zendy; Wiebcke Michael | Zendy

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Fast Nucleation and Growth of ZIF‐8 Nanocrystals Monitored by Time‐Resolved In Situ Small‐Angle and Wide‐Angle X‐Ray Scattering

Author(s) -

Cravillon Janosch,

Schröder Christian A.,

Nayuk Roman,

Gummel Jeremie,

Huber Klaus,

Wiebcke Michael

Publication year - 2011

Publication title -

angewandte chemie international edition

Language(s) - English

Resource type - Journals

SCImago Journal Rank - 5.831

H-Index - 550

eISSN - 1521-3773

pISSN - 1433-7851

DOI - 10.1002/anie.201102071

Subject(s) - nucleation , small angle x ray scattering , nanocrystal , scattering , in situ , materials science , wide angle x ray scattering , small angle scattering , optics , crystallography , molecular physics , chemical physics , analytical chemistry (journal) , nanotechnology , chemistry , small angle neutron scattering , physics , thermodynamics , neutron scattering , organic chemistry , chromatography

Prenucleation clusters : In situ synchrotron X‐ray scattering with a one‐second time resolution revealed the occurrence of nano‐sized clusters during the nucleation and early growth of nanocrystals of a zeolitic imidazolate framework (ZIF). The complex crystallization process exhibits similarities with crystallization processes of zeolites from solution. Hmim= 2‐methylimidazole.

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