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Polymer cages  prepared by etching of gold nanoparticles from polymer templates by the “grafting around” method are designed for selective separation of metal nanoparticles. The separation process is demonstrated as a fast biphasic ligand exchange reaction. The high separation efficiency and size selectivity of the polymer cage is verified by comparison with the linear block copolymer.

Polymer/Nanoparticle Hybrid Materials of Precise Dimensions by Size‐Exclusive Fishing of Metal Nanoparticles