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Graphene oxide (GO) is one of the important functional materials. Large-scalesynthesis of it is very challenging. Following a simple cost-effective route,large-scale GO was produced by mechanical (ball) milling, in air, of carbonnanoparticles (CNPs) present in carbon soot in the present study. The thicknessof the GO layer was seen to decrease with an increase in milling time. Ballmilling provided the required energy to acquire the in-plane graphitic order inthe CNPs reducing the disorders in it. As the surface area of the layeredstructure became more and more with the increase in milling time, more and moreoxygen of air got attached to the carbon in graphene leading to the formationof GO. An increase in the time of the ball mill up to 5 hours leads to asignificant increase in the content of GO. Thus ball milling can be useful toproduce large-scale two-dimensional GO for a short time.

Large scale synthesis of 2D graphene oxide by mechanical milling of 3D carbon nanoparticles in air