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We describe the development of a millifluidic based scanning droplet cellplatform for rapid and automated corrosion. This system allows for measurementof corrosion properties (e.g., open circuit potential, corrosion currentthrough Tafel and linear polarization resistance measurements, and cyclicvoltammograms) on a localized section of a planar sample. Our system is highlyautomated and flexible, allowing for scripted changing and mixing of solutionsand point-to-point motion on the sample. We have also created an automated dataanalysis pipeline. Here we demonstrate this tool by corroding a plate ofelectroplated Zn$_{85}$Ni$_{15}$ alloy over a range of pH values and correlateour results with XPS measurements and literature.

Development of an automated millifluidic platform and data-analysis pipeline for rapid electrochemical corrosion measurements: a pH study on Zn-Ni