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This article reports an easy route synthesis of bulk polycrystalline TiSe2.Phase purity and microstructure are determined through powder X-ray diffraction(PXRD) and field emission scanning electron microscopy (FESEM) respectively.Vibrational modes of TiSe2 as being analyzed by Raman spectroscopy, show theoccurrence of both Ag and Eg modes. Charge density wave (CDW) is observed intransport measurements of TiSe2 with hysteresis in cooling and warmingmeasurements at around 180K. Further, studied TiSe2 showed negativemagnetoresistance (MR) below the CDW and a small positive MR above the CDW.

Growth, structure, micro-structure and magneto transport of an easy route synthesized bulk polycrystalline TiSe2