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The search for a new energy paradigm with net-zero carbon emissions requiresnew technologies for energy generation and storage that are at the crossroadbetween engineering, chemistry, physics, surface and materials sciences. Tokeep pushing the inherent boundaries of device performance and lifetime, weneed to step away from a cook-and-look approach and aim to establish thescientific ground to guide the design of new materials. This requires strongefforts in establishing bridges between microscopy and spectroscopy techniques,across multiple scales. Here, we discuss how the complementarities of X-ray-and electron-based spectroscopies and atom probe tomography can be exploited inthe study of surfaces and sub-surfaces to understand structure-propertyrelationships in electrocatalysts.

Correlating atom probe tomography with X-Ray and electron spectroscopies to understand microstructure-activity relationships in electrocatalysts