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We propose an application of the Angular X-ray Cross-Correlation Analysis(AXCCA) to the scattered intensity distribution measured in three-dimensional(3D) reciprocal space from a single crystalline sample. Contrary to theconventional application of AXCCA, when averaging over many two-dimensional(2D) diffraction patterns collected from different randomly oriented samples isrequired, the proposed approach gives an insight into the structure of a singlespecimen. This is particularly useful in studies of defect-reach samples thatare unlikely to have the same structure. Here, we demonstrate an example of aqualitative structure determination of a colloidal crystal on the simulated aswell as experimentally measured 3D scattered intensity distributions.

Angular X-ray Cross-Correlation Analysis Applied to the Scattering Data in 3D Reciprocal Space from a Single Crystal