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The low concentration of proton donors in alkaline HER, subsequently leadingto the extra water adsorption and dissociation steps, identifies the value ofactive sites (edge and basal sites) and crystal phases in lowering the extraactivation barrier and/or optimizing the H* adsorption kinetics; in addition,the outstanding morphology-based features (surface area, thickness, defects,disorders and crystallinity) of layered molybdenum dichalcogenide familiespinpoint the roles of active sites and phases for more interpretable andfeasible structure-activity analysis. In this context, hydrothermal syntheticmethod is used to exhibit a clear mapping between the nanostructure/nanosurfacedesign and the practical HER performance by adjusting key experimentalparameters. In this article, MoX$_2$ nanostructures in different species (X =S, Se, Te), the molar ratio of added reactants (the Se metal precursor and theNaBH4 reducing agency) and hydrothermal temperature are considered for themodulated structure and the optimized HER performance.

Tunable structure-activity correlations of molybdenum dichalcogenides  (MoX$_2$; X= S, Se, Te) electrocatalysts via hydrothermal methods: insight  into optimizing the electrocatalytic performance for hydrogen generation