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The investigations of the nanostructured-Al (nano-Al) based thermo-oxidativereaction attributes are detailed in this chapter-5. Two products are selectedfor the thermo-oxidative reaction studies. They are (1) Nano-Al embedded in thePVP matrix (will be termed as fuel) and (2) its physically mixed 1:1stoichiometric nanocomposite processed with the ultrafine nc-ceria oxidizer(also will be termed as nanoenergetic material (NEM)), respectively. Thegraphical abstract presented below illustrates an overview of thethermo-oxidative reaction of fuel tracked employing thermogravimetric analysis(TGA) investigation. Similar TGA experimentation of the designed NEMs iscarried out to gather scientific information validating, whether or not adesired enhanced attribute is achieved. Also, in coincidence with the TGAoxidation event, a synchronous exothermic energy release event in differentialscanning calorimetry (DSC) trace is observed. The above mentioned two productsand their thermo-oxidative reaction behavior employing TGA/DTA and TGA/DSCthermal traces are compared and interpreted based on the data available in theliterature.

Investigation of energetics of 1:1 stoichiometric Al/PVP-fuel and nc-CeO2-oxidizer nanocomposite material