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The viability of ultrasonic sonochemistry is investigated in the context ofdelivering air-stable metallic Al rich-PVP composite. The parametersinvestigated are; sono-(1) process intensification, (2) crystallization, (3)agglomeration, and (4) fragmentation, respectively. The conventional solvent ofn-hexadecane is employed as the sonotrode generated pressure transmittingmedium to carry out the above experiments. Two precursors, (1) Poly(vinylpyrrolidone) (PVP) and (2) Aluminum chloride (AlCl3) are chosen toevaluate and demonstrate the viability of the ultrasonic induced processing.Temperature controlled investigations at RT and higher temperature help inachieving; (a) PVP-graphitization, and (b) Al-crystal growth phenomenon,respectively. The current experiments aid in helping to isolate and identifyactual mechanistic happenings. The investigation, thus, has a fabricationprotocol of shortened processing-duration, native amorphous oxide-free,metal-rich air-stable product that leads to 10 g of composite product for fuelapplications.

Viability of Ultrasonic Sonochemical processing for nanostructures: Case study of Aluminum-crystal growth and Poly (vinylpyrrolidone)-graphitization