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We report the synthesis of a bulk nanostructured alloy using the laser-powderbed fusion process. The equiatomic AlCoCrFeMnNi chemically complex alloy formsa nanoscale modulated structure, which is homogeneously distributed in theas-built condition. The nanostructure consisted of Al & Ni-rich ordered (B2)and Cr & Fe-rich disordered (A2) BCC phases. The two phases form aninterconnected phase-network with coherent interface boundaries.Atom-probe-tomography and aberration-corrected scanning transmission electronmicroscopy analysis of the spatial distribution of the modulated structuresuggests the occurrence of nano-scale spinodal decomposition. These resultsintroduce a direct synthesis of bulk nanostructured alloys with promisinggeometric flexibility.

Bulk nanostructured AlCoCrFeMnNi chemically complex alloy synthesized by laser-powder bed fusion process